【填空题】
5、标定EDTA深液时，若控制pH=5，常选用___为金属离子指示剂；若控制pH=10，常选用___为金属离子指示剂。
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【填空题】
6、测定胆矾中铜含量时，用Na2S2O3滴定至浅黄色才加入淀粉的原因是___，继续滴定至浅蓝色，加入NH4SCN的作用是___。
【填空题】
7、以NaOH标准溶液滴定HAc溶液，选择___指示剂；称取KHC8H4O4基准物质标定0.1mol/LNaOH溶液，选择___指示剂。
【填空题】
8、在邻二氮菲吸光光度法测铁含量实验中，邻二氮菲是___，盐酸羟胺的作用是___，醋酸钠的作用是___。
【填空题】
9、以KlO3为基准标定Na2S2O3溶液选择___指示剂，由___色变为___色即为终点；以Na2C2O4为基准标定KMnO4溶液以___为指示剂，由___色变为___色即为终点。
【填空题】
2、分析化学实验中所用纯水的制备方法有___、___、___。
【填空题】
3、用双盘半机械加码电光分析天平称量，在校正天平零点时___，天平应处于___状态；在加减砝码和取放被称量物时，天平应处于___状态，在试加圈码时，天平可以处于___状态；在读取称量数据时，天平应处于___状态；为加快称量速度，加减砝码的顺序___是___，判断左右两盘熟轻熟重的方法是___。用分析天平称取试样的方法有___。
【填空题】
4、具塞___滴定管用来盛装___及___溶液；碱式滴定管用来盛装___及___溶液，不宜装___溶液；滴定管在装溶液前需用待装溶液润洗___次，其目的是___。50mL滴定管的最小分度是___，如放出约5mL溶液时，记录数据为___位有效数字,相对误差为___。若使误差<0.1%，则滴定体积至少为___。
【填空题】
5、以下酸碱指示剂的pH变色范围和颜色变化分别为：甲基橙 ___、___；甲基红___、___；酚酞___、___。以下常见金属指示剂适用的pH范围和颜色变化分别为：铬黑T___ 、___、___； 二甲酚橙___、___、___；钙指示剂___、___；氧化还原指示剂二苯胺磺酸钠的条件电位和颜色变化为：___、___；莫尔法的指示剂、颜色变化、适宜酸度为___、___、___；佛尔哈德法的指示剂、颜色变化、适宜酸度为 ___、___、___。
【填空题】
8、为下列操作选择合适的容器：称取CaCO3基准物时，装CaCO3基准物用___；盛装K2Cr2O7标准溶液以进行滴定，用___；储存AgNO3标准溶液，用___；储存0.2 mol·L-1NaOH溶液，用___；
【填空题】
9、指出在不同酸度下作络合滴定时应选择的缓冲溶液 ：pH=1时EDTA滴定Bi3+ ___ ； pH=5时EDTA滴定Pb2+ ___；pH=10时EDTA滴定Mg2+ ___；pH=13时EDTA滴定Ca2+ ___。
【填空题】
分光光度法测定铁的显色剂是___，测铁的总量时需加入___
【填空题】
将Fe3+还原为Fe2+，测定时溶液的酸度宜用 ___控制pH在___左右，酸度过高则 ___，酸度过低则___。
【单选题】
使用721型分光光度计时仪器在100％处经常漂移的原因是___。
A. 保险丝断了
B. 电流表动线圈不通电
C. 稳压电源输出导线断了
D. 电源不稳定
【单选题】
可见-紫外分光度法的适合检测波长范围是___。
A. 400-760nm
B. 200-400nm
C. 200-760nm
D. 200-1000nm
【单选题】
某有色溶液在某一波长下用2cm吸收池测得其吸光度为0.750，若改用0.5cm和3cm吸收池，则吸光度各为___。
A. 0.188/1.125
B. 0.108/1.105
C. 0.088/1.025
D. 0.180/1.120
【单选题】
在分光光度法中，应用光的吸收定律进行定量分析，应采用的入射光为___。
A. 白光
B. 单色光
C. 可见光
D. 复合光
【单选题】
入射光波长选择的原则是___。
A. 吸收最大
B. 干扰最小
C. 吸收最大干扰最小
D. 吸光系数最大
【单选题】
如果样品比较复杂，相邻两峰间距离太近，保留值难以准确测量时，可采用___。
A. 相对保留值进行定性
B. 加入已知物以增加峰高的方法定性
C. 利用文献保留值定性
D. 利用检测器定性
【单选题】
洗涤被染色的吸收池，比色管，吸量管等一般使用___。
A. 肥皂
B. 铬酸洗液
C. 盐酸-乙醇洗液
D. 合成洗涤剂
【单选题】
下列分子中能产生紫外吸收的是___。
A. NaO
B. C2H2
C. CH4
D. K2O
【单选题】
在分光光度法中，宜选用的吸光度读数范围___。
A. 0～0.2
B. 0.1～∞
C. 1～2
D. 0.2～0.8
【单选题】
紫外—可见光分光光度计结构组成为___。
A. 光源-----吸收池------单色器------检测器-----信号显示系统
B. 光源-----单色器------吸收池------检测器-----信号显示系统
C. 单色器-----吸收池------光源 ------检测器-----信号显示系统
D. 光源-----吸收池------单色器------检测器
【单选题】
紫外可见分光光度计中的成套吸收池其透光率之差应为___。
A. ＜0.5%
B. ＜0.1%
C. 0.1%-0.2%
D. ＜5%
【单选题】
检查气瓶是否漏气，可采用___的方法。
A. 用手试
B. 用鼻子闻
C. 用肥皂水涂抹
D. 听是否有漏气声音
【单选题】
原子吸收分光光度计的核心部分是 ___。
A. 光源
B. 原子化器
C. 分光系统
D. 检测系统
【单选题】
氧气通常灌装在___颜色的钢瓶中
A. 白色
B. 黑色
C. 深绿色
D. 天蓝色
【单选题】
用原子吸收光谱法测定钙时，加入EDTA是为了消除___干扰。
【单选题】
原子吸收光谱是___。
A. 带状光谱
B. 线状光谱
C. 宽带光谱
D. 分子光谱
【单选题】
欲分析165～360nm的波谱区的原子吸收光谱， 应选用的光源为___。
A. 钨灯
B. 能斯特灯
C. 空心阴极灯
D. 氘灯
【单选题】
原子吸收光度法的背景干扰，主要表现为___形式。
A. 火焰中被测元素发射的谱线
B. 火焰中干扰元素发射的谱线
C. 光源产生的非共振线
D. 火焰中产生的分子吸收
【单选题】
仪器分析中标准储备溶液的浓度应不小于___。
A. 1μg/mL
B. 1mg/mL
C. 1g/mL
D. 1mg/L
【单选题】
使原子吸收谱线变宽的因素较多，其中___是最主要的。
A. 压力变宽
B. 温度变宽
C. 多普勒变宽
D. 光谱变宽
【单选题】
原子吸收光谱定量分析中，适合于高含量组分的分析的方法是___。
A. 工作曲线法
B. 标准加入法
C. 稀释法
D. 内标法
【单选题】
在原子吸收分光光度计中，若灯不发光可___。
A. 将正负极反接半小时以上
B. 用较高电压（600V以上）起辉
C. 串接2～10千欧电阻
D. 在50mA下放电
【单选题】
原子吸收光谱法中的物理干扰可用下述___的方法消除。
A. 扣除背景
B. 加释放剂
C. 配制与待测试样组成相似的溶液
D. 加保护剂
【单选题】
装在高压气瓶的出口，用来将高压气体调节到较小压力的是___。
A. 减压阀
B. 稳压阀
C. 针形阀
D. 稳流阀
【单选题】
选择不同的火焰类型主要是根据___。
A. 分析线波长
B. 灯电流大小
C. 狭缝宽度
D. 待测元素性质
【单选题】
原子吸收仪器中溶液提升喷口与撞击球距离太近，会造成下面___。
A. 仪器吸收值偏大
B. 火焰中原子去密度增大，吸收值很高
C. 雾化效果不好、噪声太大且吸收不稳定
D. 溶液用量减少
【单选题】
空心阴极灯的操作参数是___。
A. 阴极材料的纯度
B. 阳极材料的纯度
C. 正负电极之间的电压
D. 灯电流
【单选题】
由原子无规则的热运动所产生的谱线变宽称为___。
A. 自然变度
B. 赫鲁兹马克变宽
C. 劳伦茨变宽
D. 多普勒变宽
推荐试题
【单选题】
Tom is a book lover. ______ likes reading very much.
A. He B. She C. You D. It
【单选题】
—May I listen to the music here, Mr. White?
—Sorry, you’d better it like that．
A. not to do B. not do to
C. dont do D. not do
【单选题】
3.—Did you have a good time at Lauras birthday party?
— Yes, indeed. Its several years ________ I enjoyed myself so much.
A. when B. before C. since D. that
【单选题】
4. —___________ is the Summer Palace from here?
About three kilometers away. You can take the No. 35 bus.
A. How long B. How far C. How often D. How much
【单选题】
5. I was looking for a birthday gift for my mother, but I couldnt find ______ suitable.
A. anything B. something C. nothing D. everything
【单选题】
6. A friend of my ____ and I are going to visit_______ next week．
A. father; Browns B. father's; Browns
C. father; the Browns D. father's; the Browns
【单选题】
7. She ______ very hard since she came to our school.
A. studies B. has studied C. is studying D. studied
【单选题】
8. — Who will send you to the new school, your mom or your dad?
— _______. Ill go there by myself.
A. Both B. Either C. Neither D. None
【单选题】
9.—Well do what we can ____English well this term．
—It’s high time for you to work hard．
A. study B．to study C. be studied D. be studying
【单选题】
10. —I’m going to Flower Bookstore. Could you tell me ______?
— Sorry, I don’t know. I’m new here.
A. where it is B. where was it C. where is it D. where it was
【单选题】
11. How do you like the dishes, Eric?
— Fantastic! Nothing tastes ________.
A. nice B. better C. terrible D. worse
【单选题】
12. ______ Lin Feng has to work late, she always wears a smile on her face.
A. Because B. If C. Until D. Though
【单选题】
13.You can save money _______ you buy cheaper things.
A. before B. unless C. if D. until
【单选题】
14. We will have a _________ holiday after the exam．
A. two-month B. two month’s C. two month D. two-months
【单选题】
15. —We will build an underground in Xuzhou before 2015．
— Wow, _______! Will it pass our place?
A. what an excited news B. how excited the news is
C. what exciting news D. how exciting
【单选题】
16. — Emily, here’s a dictionary．I hope it will help you in some way．
— Thank you．It’s ________ what I need．
A. almost B. still C. only D. just
【单选题】
17. —Oh．I’m hungry．Mum, can I have the hamburger on the plate?
—No．It tastes ．
A. terribly B. terrible C. good D. well
【单选题】
18. —We can invite our teachers to the farewell party next Saturday.
—Yes, ______? I’ll call them at once.
A. what for B. what C. why not D. why
【单选题】
19.You can ________ ask the old man to move away to any other place because he has lived ________ here for at least sixty years．
A. hardly; alone B. hard; alone
C. hardly; lonely D. hardly; lonely
【单选题】
20.—I’m going back to see my grandparents this weekend．
—________．
A. It’s very nice of you B. You’d better hurry
C. Say goodbye to them D. Give my best wishes to them
【单选题】
21.—Why not take ____ umbrella with the sign “Made in China”? It is useful.
—What _______ good advice it is!
A. an; a B. a; a C. an; \ D. \; a
【单选题】
22. —Do you know the boy________ is sitting next to Peter?
— Yes. He is Peter’s friend. They are celebrating his ________ birthday.
A. who; ninth B. that; ninth C. /; ninth D. which; ninth
【单选题】
23. It was dark, ______ I couldnt see what was happening.
A. or B. though C. but D. so
【单选题】
24.—You can use MSN to talk with Vivien on the Internet.
—I know. But can you tell me ________?
A. what I can use it B. when I can use it
C. why can I use it D. how can I use it
【单选题】
25. _______ are you going to the School Uniform Exhibition, Amy ?
To learn about different styles of school uniform.
A. What B. Where C. Which D. Why
【单选题】
( ) 26. Where does the writer of "The little Prince" come from?
A．England． B．France． C．America． D．China．
【单选题】
( ) 27. What does the prince do after the fox tells him a secret?
A．He cares more about a flower and a sheep．
B．He meets many more strange adults on other planets．
C．He realizes his love for the rose and he goes back to his planet．
D．He discovers interesting things such as a snake, other roses and a fox
【单选题】
( ) 28. What does "The little Prince" mainly talk about? It' s about _________．
A．the adult world B．the planet B -612
C．a rose and a fox D．the adventure of a young prince
【单选题】
( ) 29. What is the writer's main purpose（目的）in writing this passage？
A．To tell the readers his life story．
B．To tell people what kind of person his father was．
C．To tell the readers what present he got from his father．
D． To let people know how poor he was．
【单选题】
( ) 30. Why did the father not ask his son not to do this and do that？
A．Because he felt quite confident of his son．
B．Because he was born from a poor family．
C．Because he was a man of few words．
D．Because he didn't want to be much too strict with his son．
【单选题】
( ) 31. What would someone learn from this passage？
A．How to live by oneself． B．How to stand on one's own feet．
C．What a good father should do． D．What the self-important is like．
【单选题】
( ) 32. What may be the proper Chinese for the underlined part in the passage？
A．闲暇时光 B．学费 C．精神空虚 D．经济不足
【单选题】
( ) 33. Why did Natalie Smith pay for the six cars behind her?
A. She had seven tickets.
B. She hoped to please others.
C. She knew the car drivers well.
D. She wanted to show kindness.
【单选题】
( ) 34. Judy Foreman copied down the phrase because she ___ .
A. thought it was beautifully written
B. wanted to know what it really meant
C. decided to write it on a warehouse wall
D. wanted her husband to put it up in the classroom
【单选题】
( ) 35. Who came up with the phrase according to the passage?
A. Judy Foreman. B. Natalie Smith. C. Anne Herbert D. Alice Johnson.
【单选题】
( ) 36. What can we infer from the last paragraph?
A. People should practice random kindness to those in need.
B. People who receive kindness are likely to offer it to others.
C. People should practice random kindness to strangers they meet.
D. People who receive kindness are likely to pay it back to the giver.
【单选题】
( ) 37.The greatest river for navigation is ___________.
A. the Nile B. the Amazon C. the Mekong D. the Mississippi
【单选题】
( ) 38. From a dam, people can use the water for ___________.
A. keeping the rivers clean B. only making electricity
C. irrigation and making electricity D. washing clothes
【单选题】
( ) 39. The water in the river is polluted because of _____________.
A. people's drinking water too much B. people's swimming in the river too much
C. chemicals and other materials D. people's building a dam across a river
【单选题】
( ) 40. The best title of the passage is ___________.
A. Rivers in Cities B. The importance of Rivers
C. Transportation D. Natural Resources
