【填空题】
5、标定EDTA深液时，若控制pH=5，常选用___为金属离子指示剂；若控制pH=10，常选用___为金属离子指示剂。
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【填空题】
6、测定胆矾中铜含量时，用Na2S2O3滴定至浅黄色才加入淀粉的原因是___，继续滴定至浅蓝色，加入NH4SCN的作用是___。
【填空题】
7、以NaOH标准溶液滴定HAc溶液，选择___指示剂；称取KHC8H4O4基准物质标定0.1mol/LNaOH溶液，选择___指示剂。
【填空题】
8、在邻二氮菲吸光光度法测铁含量实验中，邻二氮菲是___，盐酸羟胺的作用是___，醋酸钠的作用是___。
【填空题】
9、以KlO3为基准标定Na2S2O3溶液选择___指示剂，由___色变为___色即为终点；以Na2C2O4为基准标定KMnO4溶液以___为指示剂，由___色变为___色即为终点。
【填空题】
2、分析化学实验中所用纯水的制备方法有___、___、___。
【填空题】
3、用双盘半机械加码电光分析天平称量，在校正天平零点时___，天平应处于___状态；在加减砝码和取放被称量物时，天平应处于___状态，在试加圈码时，天平可以处于___状态；在读取称量数据时，天平应处于___状态；为加快称量速度，加减砝码的顺序___是___，判断左右两盘熟轻熟重的方法是___。用分析天平称取试样的方法有___。
【填空题】
4、具塞___滴定管用来盛装___及___溶液；碱式滴定管用来盛装___及___溶液，不宜装___溶液；滴定管在装溶液前需用待装溶液润洗___次，其目的是___。50mL滴定管的最小分度是___，如放出约5mL溶液时，记录数据为___位有效数字,相对误差为___。若使误差<0.1%，则滴定体积至少为___。
【填空题】
5、以下酸碱指示剂的pH变色范围和颜色变化分别为：甲基橙 ___、___；甲基红___、___；酚酞___、___。以下常见金属指示剂适用的pH范围和颜色变化分别为：铬黑T___ 、___、___； 二甲酚橙___、___、___；钙指示剂___、___；氧化还原指示剂二苯胺磺酸钠的条件电位和颜色变化为：___、___；莫尔法的指示剂、颜色变化、适宜酸度为___、___、___；佛尔哈德法的指示剂、颜色变化、适宜酸度为 ___、___、___。
【填空题】
8、为下列操作选择合适的容器：称取CaCO3基准物时，装CaCO3基准物用___；盛装K2Cr2O7标准溶液以进行滴定，用___；储存AgNO3标准溶液，用___；储存0.2 mol·L-1NaOH溶液，用___；
【填空题】
9、指出在不同酸度下作络合滴定时应选择的缓冲溶液 ：pH=1时EDTA滴定Bi3+ ___ ； pH=5时EDTA滴定Pb2+ ___；pH=10时EDTA滴定Mg2+ ___；pH=13时EDTA滴定Ca2+ ___。
【填空题】
分光光度法测定铁的显色剂是___，测铁的总量时需加入___
【填空题】
将Fe3+还原为Fe2+，测定时溶液的酸度宜用 ___控制pH在___左右，酸度过高则 ___，酸度过低则___。
【单选题】
使用721型分光光度计时仪器在100％处经常漂移的原因是___。
A. 保险丝断了
B. 电流表动线圈不通电
C. 稳压电源输出导线断了
D. 电源不稳定
【单选题】
可见-紫外分光度法的适合检测波长范围是___。
A. 400-760nm
B. 200-400nm
C. 200-760nm
D. 200-1000nm
【单选题】
某有色溶液在某一波长下用2cm吸收池测得其吸光度为0.750，若改用0.5cm和3cm吸收池，则吸光度各为___。
A. 0.188/1.125
B. 0.108/1.105
C. 0.088/1.025
D. 0.180/1.120
【单选题】
在分光光度法中，应用光的吸收定律进行定量分析，应采用的入射光为___。
A. 白光
B. 单色光
C. 可见光
D. 复合光
【单选题】
入射光波长选择的原则是___。
A. 吸收最大
B. 干扰最小
C. 吸收最大干扰最小
D. 吸光系数最大
【单选题】
如果样品比较复杂，相邻两峰间距离太近，保留值难以准确测量时，可采用___。
A. 相对保留值进行定性
B. 加入已知物以增加峰高的方法定性
C. 利用文献保留值定性
D. 利用检测器定性
【单选题】
洗涤被染色的吸收池，比色管，吸量管等一般使用___。
A. 肥皂
B. 铬酸洗液
C. 盐酸-乙醇洗液
D. 合成洗涤剂
【单选题】
下列分子中能产生紫外吸收的是___。
A. NaO
B. C2H2
C. CH4
D. K2O
【单选题】
在分光光度法中，宜选用的吸光度读数范围___。
A. 0～0.2
B. 0.1～∞
C. 1～2
D. 0.2～0.8
【单选题】
紫外—可见光分光光度计结构组成为___。
A. 光源-----吸收池------单色器------检测器-----信号显示系统
B. 光源-----单色器------吸收池------检测器-----信号显示系统
C. 单色器-----吸收池------光源 ------检测器-----信号显示系统
D. 光源-----吸收池------单色器------检测器
【单选题】
紫外可见分光光度计中的成套吸收池其透光率之差应为___。
A. ＜0.5%
B. ＜0.1%
C. 0.1%-0.2%
D. ＜5%
【单选题】
检查气瓶是否漏气，可采用___的方法。
A. 用手试
B. 用鼻子闻
C. 用肥皂水涂抹
D. 听是否有漏气声音
【单选题】
原子吸收分光光度计的核心部分是 ___。
A. 光源
B. 原子化器
C. 分光系统
D. 检测系统
【单选题】
氧气通常灌装在___颜色的钢瓶中
A. 白色
B. 黑色
C. 深绿色
D. 天蓝色
【单选题】
用原子吸收光谱法测定钙时，加入EDTA是为了消除___干扰。
【单选题】
原子吸收光谱是___。
A. 带状光谱
B. 线状光谱
C. 宽带光谱
D. 分子光谱
【单选题】
欲分析165～360nm的波谱区的原子吸收光谱， 应选用的光源为___。
A. 钨灯
B. 能斯特灯
C. 空心阴极灯
D. 氘灯
【单选题】
原子吸收光度法的背景干扰，主要表现为___形式。
A. 火焰中被测元素发射的谱线
B. 火焰中干扰元素发射的谱线
C. 光源产生的非共振线
D. 火焰中产生的分子吸收
【单选题】
仪器分析中标准储备溶液的浓度应不小于___。
A. 1μg/mL
B. 1mg/mL
C. 1g/mL
D. 1mg/L
【单选题】
使原子吸收谱线变宽的因素较多，其中___是最主要的。
A. 压力变宽
B. 温度变宽
C. 多普勒变宽
D. 光谱变宽
【单选题】
原子吸收光谱定量分析中，适合于高含量组分的分析的方法是___。
A. 工作曲线法
B. 标准加入法
C. 稀释法
D. 内标法
【单选题】
在原子吸收分光光度计中，若灯不发光可___。
A. 将正负极反接半小时以上
B. 用较高电压（600V以上）起辉
C. 串接2～10千欧电阻
D. 在50mA下放电
【单选题】
原子吸收光谱法中的物理干扰可用下述___的方法消除。
A. 扣除背景
B. 加释放剂
C. 配制与待测试样组成相似的溶液
D. 加保护剂
【单选题】
装在高压气瓶的出口，用来将高压气体调节到较小压力的是___。
A. 减压阀
B. 稳压阀
C. 针形阀
D. 稳流阀
【单选题】
选择不同的火焰类型主要是根据___。
A. 分析线波长
B. 灯电流大小
C. 狭缝宽度
D. 待测元素性质
【单选题】
原子吸收仪器中溶液提升喷口与撞击球距离太近，会造成下面___。
A. 仪器吸收值偏大
B. 火焰中原子去密度增大，吸收值很高
C. 雾化效果不好、噪声太大且吸收不稳定
D. 溶液用量减少
【单选题】
空心阴极灯的操作参数是___。
A. 阴极材料的纯度
B. 阳极材料的纯度
C. 正负电极之间的电压
D. 灯电流
【单选题】
由原子无规则的热运动所产生的谱线变宽称为___。
A. 自然变度
B. 赫鲁兹马克变宽
C. 劳伦茨变宽
D. 多普勒变宽
推荐试题
【单选题】
This kind of exercise will ___ your creativity, renew your energy, and unlock your potential.
A. bind
B. yield
C. embrace
D. stimulate
【单选题】
I’ll be happy to help you, ___ you won’t take up too much of my time.
A. as well as
B. as long as
C. as far as
D. as soon as
【单选题】
We teachers do not consider it wise to ___ our students with all sorts of exams, tests and quizzes.
A. load
B. annoy
C. sample
D. explore
【单选题】
He makes his students ___ knowledge through various kinds of interesting activities.
A. study
B. learn
C. achieve
D. acquire
【单选题】
For years, scientists have debated the ___ dangers of building another nuclear plant after the terrible accident.
A. available
B. potential
C. fascinating
D. genuine
【单选题】
It was a worthwhile attempt ___ it failed to achieve its purpose that we had hoped for.
A. in the end
B. now that
C. all at once
D. even though
【单选题】
Travel in space can be very exciting; ___, it can also be boring and lonely at times.
A. so
B. however
C. thus
D. therefore
【单选题】
Politicians should not ___ in business affairs that might affect their political judgment.
A. engage
B. embrace
C. depart
D. treasure
【单选题】
I wish to ___ a master’s degree in electric engineering after I graduate from college.
A. pledge
B. explore
C. pursue
D. approach
【单选题】
There is no greater importance ___ cultivating independence in children.
A. in
B. than
C. of
D. with
【单选题】
He has made it very clear ___ we should observe the new rules.
A. what
B. which
C. those
D. that
【单选题】
It was when I read his letter ___ I realized he had given me huge help.
A. that
B. then
C. before
D. after
【单选题】
Don’t worry too much, Jane. Your son ___ home already. Let’s go back and check it out.
A. returned
B. will return
C. has returned
D. may have returned
【单选题】
I believe friendship is an essential element of making a healthy, ___ life.
A. flexible
B. rewarding
C. wealthy
D. inquisitive
【单选题】
___ they have written about the behaviors of animals is hardly anything new.
A. That
B. This
C. What
D. Which
【单选题】
No other drugs are as good as this one; it must have been based on a(n) ___ formula (配方).
A. enormous
B. stimulating
C. unique
D. overwhelming
【单选题】
Mothers tend to be too ___ toward their children. They should let them see more of the worl D.
A. hopeful
B. protective
C. modest
D. encouraging
【单选题】
The investigation ___ evidence of a large-scale illegal trade in wild birds.
A. uncovered
B. outweighed
C. overwhelmed
D. evolved
【单选题】
Poor Laura! I feel so sorry for her. When she fell, she hurt her arm and, ___, broke her glasses.
A. in advance
B. in addition
C. over time
D. on the other hand
【单选题】
Showing some sense of humor can be a(n) ___ way to deal with some stressful situations.
A. genuine
B. available
C. effective
D. favorite
【单选题】
It will be worth the efforts even if you fail; the rewards you ___ will be great.
A. reap
B. boast
C. assure
D. cultivate
【单选题】
He suggested transporting the supplies by air. But it is absolutely ___, for it will cost too much.
A. unusual
B. uncertain
C. impractical
D. impressive
【单选题】
The newspaper didn’t mention the ___ of the damage caused by the fire.
A. range
B. level
C. extent
D. quantity
【单选题】
Do you ___ her novels as serious literature or as mere entertainment?
A. classify
B. notify
C. simplify
D. justify
【单选题】
He doesn’t ___ of buying a house this year because the bank has refused to lend him any money.
A. afford
B. make the most
C. run out
D. stand a chance
【单选题】
If you don’t ___ cooking today, we can go out to eat at the new restaurant.
A. would like
B. go on with
C. feel like
D. figure out、
【单选题】
Bullying (恃强欺弱) can ___ a climate of fear and anxiety in school, and prevent students from focusing on their schoolwork.
A. keep back
B. give rise to
C. feel like
D. make use of
【单选题】
Science can now ___ many things which were thought to be mysterious by ancient people.
A. care for
B. lay out
C. account for
D. set up
【单选题】
The school has ___ many after-class activity groups for the pupils to make their spare time more colorful.
A. set up
B. set off
C. set out
D. set down
【单选题】
When he was a small kid, he ___ from his peers because he could read fast and remember whatever he rea D.
A. showed off
B. worked out
C. stood out
D. straightened up
【单选题】
The fall in the number of deaths from heart disease is generally ___ improvements in diet.
A. put up with
B. attributed to
C. added to
D. replaced with
【单选题】
We can be partners for now, but ultimately you have to ___ to develop a new software for our project.
A. keep up
B. fire off
C. make sense
D. take the lead
【单选题】
Emotional Intelligence (情商) could be of practical use in many ___ such as how companies decide which job applicant to hire, how parents should raise their children, how schools should teach the students, and so on.
A. aspects
B. disciplines
C. structures
D. opportunities
【单选题】
The teacher should praise students for their correct answers and also suggest ___ possibilities.
A. unlimited
B. unique
C. alternative
D. essential
【单选题】
In some classrooms, desks are arranged in a U-shape, so the teacher can ___ easily with the students.
A. interrupt
B. interact
C. interpret
D. interview
【单选题】
Computer technology ___ individuals to educate themselves and adapt to a constantly changing job market.
A. lets
B. makes
C. enables
D. provides
【单选题】
Our hope for an enjoyable dinner was instantly ___ when the waiter dropped a salad plate on my hea D.
A. spoiled
B. restricted
C. exploded
D. vanished
【单选题】
___ the world has ever seen has occurred in the information and communications technologies.
A. Great a change
B. The great change
C. A greatest change
D. The greatest change
【单选题】
___ so many people around, it wasn’t convenient to have a long talk with him.
A. As
B. When
C. With
D. Since
【单选题】
Alice used to be terribly shy, but working abroad for a year has completely ___ her.
A. solved
B. transformed
C. characterized
D. regulated
