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【单选题】
1.一种钠盐可溶于水,该盐溶液加入HCl溶液后,有刺激性气体产生,同时有黄色沉淀生成,该盐是:
A. Na2S
B. Na2CO3
C. Na2SO3
D. Na2S2O3
【单选题】
2.将BaSO4和PbSO4分离开,宜采用
A. NH3H2O
B. HCl
C. H2S
D. NH4Ac
【单选题】
3.下列设备中,哪一种最适宜于测定原子量?
A. 威尔逊云室
B. 电子显微镜
C. X-射线衍射仪
D. 质谱仪
【单选题】
4.王水的成分是下列哪一种混合而成(体积比)?
A. HNO3+H2SO4(1:3)
B. H2SO4+HCl(3:1)
C. HNO3+HCl(3:1)
D. HCl+HNO3 (3:1)
【单选题】
5.微量成分是指被测组分的含量为?
A. >1%
B. <0.01%
C. 0.01%-1%
D. 0.01%-0.001%
【单选题】
6.常量滴定管可估计到±0.01mL,若要求滴定的相对误差小于0.1%,在滴定时,耗用体积控制在:
A. 10-20mL
B. 20-30mL
C. 30-40mL
D. 40-50mL
【单选题】
7.某溶液为无色,下列何种离子不能否定?
A. Ni2+
B. Mn2+
C. Cr3+
D. Co2+
【单选题】
8.KMnO4能稳定存在于何处?
A. 空气中
B. HCl
C. 碱液中
D. 稀H2SO4溶液中
【单选题】
9.用蒸馏操作分离混合物的基本依据是下列性质的哪种差异?
A. 密度
B. 挥发度
C. 溶解度
D. 化学性质
【单选题】
10.在分光光度中,浓度测量的相对误差较小(<4%)的光度范围是:
A. 0.1-0.2
B. 0.2-0.7
C. 0.8-1.0
D. 1.1-1.2
【单选题】
11.下列哪种氢氧化物既溶于NaOH,又溶于NH3•H2O
A. Al(OH)3
B. Zn(OH)2
C. Cd(OH)2
D. Ni(OH)2
【单选题】
12.1:1HCl的物质的量浓度为多少?
A. 2mol/L
B. 4mol/L
C. 6mol/L
D. 8mol/L
【单选题】
13.用紫外分光光度计可测定什么光谱?
A. 原子发射光谱
B. 分子吸收光谱
C. 电子吸收光谱
D. 原子吸收光谱
【单选题】
14.以下说法不正确的有:
A. 提纯多硝基化合物通常不采用蒸馏操作
B. 减压蒸馏能用来分离固体混合物
C. 在测熔点时,通常在接近熔点时要求升温低于1℃/min
D. 液体有机物干燥完全与否可根据是否由浑浊变澄清来判断
【单选题】
15.实验室中熔化苛性钠,选用哪种坩锅?
A. 石英坩埚
B. 瓷坩埚
C. 玻璃坩埚
D. 镍坩埚
【单选题】
16.以下说法不正确的有:
A. 提纯物经重结晶操作纯度不一定变好
B. 分液漏斗中的下层液体应从下口放出
C. 在薄层色谱实验中,点样后应使样点溶剂挥发后再放入展开剂中展开
D. 活性炭通常在非极性溶剂中的脱色效果较好
【单选题】
17.有一种白色硝酸盐固体,溶于水后,用下列试剂分别处理:① 加HCl生成白色沉淀;② 加H2SO4析出白色沉淀;③ 加氨水后析出白色沉淀,但不溶于过量氨水,这种硝酸盐的阳离子是:
A. Ag+
B. Ba2+
C. Hg2+
D. Pb2+
【单选题】
18.在蒸馏操作中,对温度计位置描述正确的是:
A. 温度计水银球的上端与蒸馏头支管下侧相平
B. 温度计水银球的中心处与蒸馏头支管口的中心位置一致
C. 温度计水银球的中心处与蒸馏头支管口下侧相平
D. 温度计水银球的上端与蒸馏头支管口的中心位置一致
【单选题】
19.欲使滤纸紧贴于布氏漏斗内,滤纸的大小应服从下列哪种原则?
A. 大于漏斗内径
B. 与漏斗内径相同
C. 略小于漏斗内径
D. 随便只要压紧漏斗即可
【单选题】
20.以下说法不正确的有:
A. 薄板制备时,需将溶剂逐渐加入到吸附剂中,边加边搅拌
B. 活性炭脱色时,活性炭加入后一般需要煮沸5-10分钟
C. 在蒸馏操作中,被蒸馏液体的量一般以圆底瓶体积的1/3~2/3为宜
D. 在加热回流时,上升蒸汽的高度一般不超过冷凝管高度的1/3
【单选题】
四氯化碳作为灭火剂是较好的,但有缺点,因为它在使用时会产生一种有毒气体,该气体是:___
A. CHCl3
B. CH2Cl2
C. CH2=CHCl
D. COCl2
【单选题】
符合比移值(R f值)的定义是:___
A. 起始点到溶剂前沿的距离与起始点到斑点中心距离的比值
B. 起始点到斑点中心距离与起始点到溶剂前沿的距离的比值
C. 起始点到斑点中心距离与斑点中心到溶剂前沿的距离的比值
D. 斑点中心到溶剂前沿的距离与起始点到斑点中心距离的比值
【单选题】
使用氢氟酸时,下列哪一个操作是不正确的?___
A. 操作应在通风厨中进行
B. 用量筒量取氢氟酸,倒入烧杯中
C. 操作上应戴上橡皮手套
D. 使用时应采用塑料或铂制器皿
【单选题】
应用酯化反应制备羧酸酯时,主要可以采用以下哪些方法提高反应的得率___
A. 提高反应的温度,延长反应的时间
B. 某一反应物过量,利用分水器分出水
C. 增加催化剂酸的用量,利用分水器分出水
D. 提高反应的温度,利用分水器分出酯
【单选题】
用布氏漏斗和吸滤瓶接抽水泵过滤沉淀后,正确的操作时哪一种?___
A. 先关水龙头,拔下抽滤瓶上的橡皮管,在取下布氏漏斗
B. 先取下布氏漏斗,再关上水龙头
C. 先拔下抽滤瓶上橡皮管,关上水龙头
D. 先把沉淀和滤纸一起取出,再关上水龙头
【单选题】
减压蒸馏结束时,正确的操作是:___
A. 关闭冷却水,移走热源,毛细管通大气和打开缓冲瓶,关闭真空泵
B. 移走热源,关闭冷却水,关闭真空泵,毛细管通大气和打开缓冲瓶
C. 移走热源,关闭冷却水,毛细管通大气和打开缓冲瓶,关闭真空泵
D. 关闭冷却水,毛细管通大气和打开缓冲瓶,移走热源,关闭真空泵
【单选题】
实验室常用的马弗炉,使用最高温度应为多少?___
A. 800℃
B. 950℃
C. 1350℃
D. 1700℃
【单选题】
进行简单蒸馏操作时发现忘加了沸石,应该:___
A. 停止加热后,马上加入沸石
B. 关闭冷却水后,加入沸石即可
C. 停止加热后,待体系充分冷却,再加入沸石
D. 不需停止加热和关闭冷却水,即可加入沸石
【单选题】
水银的温度计最广可测下列哪种温度范围 :___
A. 37℃以下
B. 100℃以下
C. 400℃以下
D. 500℃以下。
【单选题】
用毛细管法测定有机固体物质的熔点时,一般向毛细管中填充:___
A. 1mm样品
B. 2~3 mm样品
C. 2~4 cm样品
D. 1 cm样品
【单选题】
用毛细管法测定有机固体物质的熔点时,一般向毛细管中填充:___
A. 1mm样品
B. 2~3mm样品
C. 2~4cm样品
D. 1cm样品。
【单选题】
通常我们把真空压力范围划分为:粗、次高和高真空三个档次,次高真空的范围是:___
A. 0.001~10mmHg
B. 1~10mmHg
C. 10~100mmHg
D. 0.001~1mmHg
【单选题】
试管内壁上附着的少量硫,用水不能洗去时,可选用下列哪种试剂洗涤:___
A. HCl
B. HNO3
C. H3PO4
D. NH3水
【单选题】
通过简单蒸馏方法能较好地分离两种不共沸的有机物,要求这两种化合物的沸点相差不小于:___
A. 10℃
B. 20℃
C. 30℃
D. 40℃
【单选题】
在水溶液中欲析出较好的结晶,宜采用下列哪个条件?___
A. 溶液浓度很大
B. 迅速冷却
C. 用力搅拌
D. 浓度适宜,缓慢降温
【单选题】
纯化石油醚时,依次用浓硫酸、酸性高锰酸钾水溶液洗涤,其目的是:___
A. 将石油醚中的不饱和烃类除去
B. 将石油醚中的低沸点的醚类除去;
C. 将石油醚中的醇类除去
D. 将石油醚中的水份除去。
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【单选题】
Tom is a book lover. ______ likes reading very much. A. He B. She C. You D. It
A. A
B. B
C. C
D. D
【单选题】
—May I listen to the music here, Mr. White? —Sorry, you’d better it like that. A. not to do B. not do to C. dont do D. not do
A. A
B. B
C. C
D. D
【单选题】
3.—Did you have a good time at Lauras birthday party? — Yes, indeed. Its several years ________ I enjoyed myself so much. A. when B. before C. since D. that
A. A
B. B
C. C
D. D
【单选题】
4. —___________ is the Summer Palace from here? About three kilometers away. You can take the No. 35 bus. A. How long B. How far C. How often D. How much
A. A
B. B
C. C
D. D
【单选题】
5. I was looking for a birthday gift for my mother, but I couldnt find ______ suitable. A. anything B. something C. nothing D. everything
A. A
B. B
C. C
D. D
【单选题】
6. A friend of my ____ and I are going to visit_______ next week. A. father; Browns B. father's; Browns C. father; the Browns D. father's; the Browns
A. A
B. B
C. C
D. D
【单选题】
7. She ______ very hard since she came to our school. A. studies B. has studied C. is studying D. studied
A. A
B. B
C. C
D. D
【单选题】
8. — Who will send you to the new school, your mom or your dad? — _______. Ill go there by myself. A. Both B. Either C. Neither D. None
A. A
B. B
C. C
D. D
【单选题】
9.—Well do what we can ____English well this term. —It’s high time for you to work hard. A. study  B.to study  C. be studied   D. be studying
A. A
B. B
C. C
D. D
【单选题】
10. —I’m going to Flower Bookstore. Could you tell me ______? — Sorry, I don’t know. I’m new here. A. where it is B. where was it C. where is it D. where it was
A. A
B. B
C. C
D. D
【单选题】
11. How do you like the dishes, Eric? — Fantastic! Nothing tastes ________. A. nice B. better C. terrible D. worse
A. A
B. B
C. C
D. D
【单选题】
12. ______ Lin Feng has to work late, she always wears a smile on her face. A. Because B. If C. Until D. Though
A. A
B. B
C. C
D. D
【单选题】
13.You can save money _______ you buy cheaper things. A. before B. unless C. if D. until
A. A
B. B
C. C
D. D
【单选题】
14. We will have a _________ holiday after the exam. A. two-month B. two month’s C. two month D. two-months
A. A
B. B
C. C
D. D
【单选题】
15. —We will build an underground in Xuzhou before 2015. — Wow, _______! Will it pass our place? A. what an excited news B. how excited the news is C. what exciting news D. how exciting
A. A
B. B
C. C
D. D
【单选题】
16. — Emily, here’s a dictionary.I hope it will help you in some way. — Thank you.It’s ________ what I need. A. almost B. still C. only D. just
A. A
B. B
C. C
D. D
【单选题】
17. —Oh.I’m hungry.Mum, can I have the hamburger on the plate? —No.It tastes . A. terribly B. terrible C. good D. well
A. A
B. B
C. C
D. D
【单选题】
18. —We can invite our teachers to the farewell party next Saturday. —Yes, ______? I’ll call them at once. A. what for B. what C. why not D. why
A. A
B. B
C. C
D. D
【单选题】
19.You can ________ ask the old man to move away to any other place because he has lived ________ here for at least sixty years. A. hardly; alone B. hard; alone C. hardly; lonely D. hardly; lonely
A. A
B. B
C. C
D. D
【单选题】
20.—I’m going back to see my grandparents this weekend. —________. A. It’s very nice of you B. You’d better hurry C. Say goodbye to them D. Give my best wishes to them
A. A
B. B
C. C
D. D
【单选题】
21.—Why not take ____ umbrella with the sign “Made in China”? It is useful. —What _______ good advice it is!    A. an; a B. a; a C. an; \ D. \; a
A. A
B. B
C. C
D. D
【单选题】
22. —Do you know the boy________ is sitting next to Peter? — Yes. He is Peter’s friend. They are celebrating his ________ birthday. A. who; ninth B. that; ninth C. /; ninth D. which; ninth
A. A
B. B
C. C
D. D
【单选题】
23. It was dark, ______ I couldnt see what was happening. A. or B. though C. but D. so
A. A
B. B
C. C
D. D
【单选题】
24.—You can use MSN to talk with Vivien on the Internet. —I know. But can you tell me ________? A. what I can use it B. when I can use it C. why can I use it D. how can I use it
A. A
B. B
C. C
D. D
【单选题】
25. _______ are you going to the School Uniform Exhibition, Amy ? To learn about different styles of school uniform. A. What B. Where C. Which D. Why
A. A
B. B
C. C
D. D
【单选题】
( ) 26. Where does the writer of "The little Prince" come from? A.England. B.France. C.America. D.China.
A. A
B. B
C. C
D. D
【单选题】
( ) 27. What does the prince do after the fox tells him a secret? A.He cares more about a flower and a sheep. B.He meets many more strange adults on other planets. C.He realizes his love for the rose and he goes back to his planet.   D.He discovers interesting things such as a snake, other roses and a fox
A. A
B. B
C. C
D. D
【单选题】
( ) 28. What does "The little Prince" mainly talk about? It' s about _________. A.the adult world B.the planet B -612 C.a rose and a fox D.the adventure of a young prince
A. A
B. B
C. C
D. D
【单选题】
( ) 29. What is the writer's main purpose(目的)in writing this passage?    A.To tell the readers his life story.    B.To tell people what kind of person his father was.    C.To tell the readers what present he got from his father.    D. To let people know how poor he was.
A. A
B. B
C. C
D. D
【单选题】
( ) 30. Why did the father not ask his son not to do this and do that?    A.Because he felt quite confident of his son.    B.Because he was born from a poor family.    C.Because he was a man of few words.    D.Because he didn't want to be much too strict with his son.
A. A
B. B
C. C
D. D
【单选题】
( ) 31. What would someone learn from this passage?    A.How to live by oneself. B.How to stand on one's own feet.    C.What a good father should do. D.What the self-important is like.
A. A
B. B
C. C
D. D
【单选题】
( ) 32. What may be the proper Chinese for the underlined part in the passage?    A.闲暇时光 B.学费 C.精神空虚 D.经济不足
A. A
B. B
C. C
D. D
【单选题】
( ) 33. Why did Natalie Smith pay for the six cars behind her? A. She had seven tickets. B. She hoped to please others. C. She knew the car drivers well. D. She wanted to show kindness.
A. A
B. B
C. C
D. D
【单选题】
( ) 34. Judy Foreman copied down the phrase because she ___ . A. thought it was beautifully written B. wanted to know what it really meant C. decided to write it on a warehouse wall D. wanted her husband to put it up in the classroom
A. A
B. B
C. C
D. D
【单选题】
( ) 35. Who came up with the phrase according to the passage? A. Judy Foreman. B. Natalie Smith. C. Anne Herbert D. Alice Johnson.
A. A
B. B
C. C
D. S
【单选题】
( ) 36. What can we infer from the last paragraph? A. People should practice random kindness to those in need. B. People who receive kindness are likely to offer it to others. C. People should practice random kindness to strangers they meet. D. People who receive kindness are likely to pay it back to the giver.
A. A
B. B
C. C
D. D
【单选题】
( ) 37.The greatest river for navigation is ___________. A. the Nile B. the Amazon C. the Mekong D. the Mississippi
A. A
B. B
C. C
D. D
【单选题】
( ) 38. From a dam, people can use the water for ___________. A. keeping the rivers clean B. only making electricity C. irrigation and making electricity D. washing clothes
A. A
B. B
C. C
D. D
【单选题】
( ) 39. The water in the river is polluted because of _____________. A. people's drinking water too much B. people's swimming in the river too much C. chemicals and other materials D. people's building a dam across a river
A. A
B. B
C. C
D. D
【单选题】
( ) 40. The best title of the passage is ___________. A. Rivers in Cities B. The importance of Rivers C. Transportation D. Natural Resources
A. A
B. B
C. C
D. D
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